3 Nitrobenzotrifluoride
Fluoride
3-Nitrobenzotrifluoride
Chemical Formula C7H4F3NO2
Molar Mass 191.107 g/mol
Appearance Colorless to pale yellow liquid
Boiling Point 202 - 204 °C
Melting Point -29 °C
Density 1.403 g/cm³ at 20 °C
Vapor Pressure 0.2 mmHg at 25 °C
Solubility In Water Insoluble
Flash Point 88 °C
Refractive Index 1.4735 at 20 °C
FAQ

What are the main uses of 3-nitrotrifluorotoluene?

3-Hydroxypropyl triethoxysilane, its main uses are wide. In the field of construction, it can be used as a concrete sealant. It can penetrate into the interior of concrete, react with its chemical composition, generate insoluble substances, fill pores, enhance compactness, improve impermeability, waterproof and moisture-proof, resist rainwater and groundwater erosion, and prolong building life. Such as ancient building restoration, it is used for masonry waterproofing to prevent structural damage due to water erosion.

In the coating industry, it is an excellent adhesion promoter. It can react with the resin in the coating and the hydroxyl group on the surface of the substrate to form chemical bonds, enhance the bonding force between the coating and the substrate, make the coating firmer, not easy to fall off and peel, and improve the durability and protective performance of the coating. It is suitable for coating various materials such as metal, wood, and plastic.

In the manufacture of composite materials, as a coupling agent, it connects inorganic materials (such as glass fibers, talc powder) and organic polymer matrices. One end reacts with the hydroxyl group on the surface of inorganic materials, and the other end reacts with organic polymers to enhance the interfacial bonding force between the two and improve the mechanical properties of composites, such as strength, toughness, heat resistance, etc., which are widely used in aerospace, automobile manufacturing and other fields.

In the textile industry, fabrics can be functionally finished. Gives fabrics water and oil repellent properties, reducing liquid adsorption and penetration; improves fabric feel, making them soft and smooth; also improves fabric antistatic properties and reduces electrostatic accumulation. Treated fabrics are more comfortable, durable and have special functions. < Br >
In electronic packaging materials, it enhances the bonding between fillers and polymer matrices, improves the electrical and mechanical properties of materials, and meets the needs of miniaturization and high performance of electronic equipment to ensure the stable operation of electronic components.

What are the physical properties of 3-nitrotrifluorotoluene?

3-Carboxytriethylamine salt is a genus of organic compounds. Its physical properties are particularly important and are described as follows:

Under normal temperature and pressure, it often takes the form of a colorless to light yellow transparent liquid. Its texture is uniform and its fluidity is quite good. There is no significant precipitation or suspended solids. It is clear in appearance. This state is convenient for many experiments and industrial operations such as dumping and transfer.

Smell its smell, with a special amine smell. Although it is not very strong and pungent, it is also clearly identifiable. This odor feature can be used as a preliminary identification of the substance. < Br >
When it comes to solubility, it exhibits good solubility in water and can be miscible with water in any ratio. Due to the structural characteristics of carboxyl groups and triethylamine salts, it can form hydrogen bonds with water molecules and interact with them. It also has good solubility in common organic solvents, such as ethanol and acetone. This property makes it an excellent reaction medium or intermediate for participating in reactions in organic synthesis reactions, providing a convenient environment for various chemical reactions.

When it comes to melting point and boiling point, the melting point is relatively low, and it is liquid at room temperature. This characteristic makes it unnecessary to heat and melt complex steps during operation. The boiling point varies according to the specific chemical structure and purity. Generally speaking, it is in a specific temperature range. This temperature range is of key guiding significance for its separation, purification and reaction applications under different temperature conditions.

As for the density, it is slightly higher than that of water, so that when it is mixed with water, if it is left to stand and stratify, it will be in the lower layer. This density characteristic can be used as an important reference in the process of material separation and identification.

In addition, its stability is acceptable under normal conditions. However, in the case of extreme chemical environments such as strong acids and bases, or special conditions such as high temperatures and strong oxidizers, chemical reactions may occur, causing changes in its structure and properties. Therefore, when storing and using, it is necessary to properly select the appropriate environment and method according to its physical properties to ensure its stability and application safety.

What are the chemical properties of 3-nitrotrifluorotoluene?

3-Carboxyl triethoxysilane has unique chemical properties. Its properties can bridge the gap between organic and inorganic, just like a clever craftsman who connects the two.

In this substance, the carboxyl group is an active group and is acidic. It can react with bases to form salts; it can also react with alcohols under acid catalysis to perform esterification, and raw esters and water. It is like an ancient craftsman who used ingenuity to combine two materials to form new substances.

Triethoxysilane group, in which the ethoxy group has the property of hydrolysis. When exposed to water, it is as if it has changed, and the ethoxy group gradually separates from the silicon atom, the hydrogenic alcohol and the silanol group. The silanol group has strong activity and can be condensed with other silanol groups to form a siloxane structure. This process is like a sand-forming tower, and the structure is gradually complex and firm.

And 3-carboxyl triethoxysilane is also modified on the surface of the material. With its treatment of the surface of the material, the carboxyl group is combined with the surface active check point, and the ethoxy group is hydrolyzed and condensed to form a siloxane film on the surface. The film changes the surface properties, or increases the hydrophilicity, or has strong corrosion resistance, and is suitable for the material to coat and increase its performance.

And because it can participate in the polymerization reaction, it can add energy to the polymerization system. Both carboxyl and ethoxy groups can be used as the check point of the reaction, connecting the monomers to form polymers with special structures and properties. In various fields, such as coatings, adhesives, composites, etc., they all develop their strengths and contribute to the prosperity of various industries, such as the stars shining in the sky, illuminating the way to help the industry.

What is the preparation method of 3-nitrotrifluorotoluene?

3-Hydroxypropyl triethoxysilane. To prepare this product, the method is as follows:

First take an appropriate amount of trichlorosilane and place it in a special reactor. The kettle needs to be pre-filled with dried nitrogen to remove moisture and impurities and create an oxygen-free and anhydrous environment. After the nitrogen is introduced for a while, slowly add an appropriate amount of allyl alcohol, and closely monitor the reaction temperature. Use an ice-water bath or other temperature control means to ensure that the reaction temperature is maintained between 20 and 30 degrees Celsius. During this reaction, trichlorosilane and allyl alcohol undergo an addition reaction to form the intermediate chloropropyl trichlorosilane.

After the addition reaction is almost complete, the temperature of the reaction system is gradually increased to 60 to 70 degrees Celsius after confirming the degree of reaction by chemical analysis. Then, an appropriate amount of ethanol-diluted absolute sodium ethanol solution is slowly added to it to initiate a substitution reaction. Sodium ethanol is substituted with the chlorine atom in the intermediate to generate 3-hydroxypropyl triethoxysilane. During the reaction, stirring is continued to fully contact the reactants and accelerate the reaction process.

After the reaction is completed, the system is cooled to room temperature, and the reaction mixture is moved into the separation funnel. Extract with an appropriate amount of organic solvent such as ether, and after multiple extractions, combine the organic phases. Then dry the organic phase with anhydrous magnesium sulfate to remove moisture. After drying, the organic solvent and unreacted raw materials are removed by vacuum distillation, and the fractions within the corresponding boiling point range are collected to obtain 3-hydroxypropyl triethoxysilane with high purity. The entire preparation process requires strict adherence to operating procedures, attention to safety protection, and precise control of the reaction conditions and material dosage of each step to obtain satisfactory products.

What are the precautions for the storage and transportation of 3-nitrotrifluorotoluene?

3-Hydroxypropyl triethoxysilane is in storage and transportation, and all kinds of precautions are essential.

This agent is volatile and flammable. Therefore, in the storage place, it must be kept away from fire and heat sources to prevent the invasion of open flames and prevent the risk of fire. The ambient temperature should also be properly controlled and not too high, so as not to accelerate volatilization or cause other accidents. It is advisable to choose a cool, dry and well-ventilated place, so as to ensure the stability of its chemical properties.

The packaging must be tight and leak-free. Due to its chemical properties, if the package is damaged and leaks, it will not only lose materials, but also react with surrounding substances, causing danger. And because it may be corrosive to some materials, the choice of packaging materials should be cautious, generally corrosion-resistant materials are appropriate.

When transporting, do not slack off. Transportation vehicles need to be equipped with corresponding fire equipment and leakage emergency treatment equipment for emergencies. During transportation, ensure that the container is stable and does not collide, dump, or cause damage to the package. Drivers and escorts should also be familiar with its hazard characteristics and emergency disposal methods, and transportation route planning should also avoid densely populated areas and important places.

In addition, whether it is storage or transportation, relevant laws and standards must be strictly followed. The person handling this agent should also receive professional training, be familiar with the operating procedures, and take personal protection during operation, such as wearing appropriate protective gloves, protective glasses, etc., to prevent physical damage from contact. In this way, the safety of 3-hydroxypropyl triethoxysilane during storage and transportation must be ensured.